Preparation of Different Topography NiCo2O4 with Surfactant by Solid

doi:10.3724/SP.J.1077.2007.00040

Abstract

Abstract: Manifold mixed precursors were prepared with Ni(CH₃COO)₂·4H₂O, Co(CH₃COO)₂·4H₂O, H₂C₂O₄·2H₂O and different surfactants by solid state reaction at room temperature; then they were put into a bain-marie to keep 2d at 60℃. After these precursors analyzed by TG-DTA, and decomposed at 610℃, the phase and topography of the thermolysis products were characterized by XRD, SEM. The nanometer composite oxide NiCo₂O₄ with different topography was obtained. The experimental results show that these surfactants act as soft-templates, they have evident effect on topography of products.

Key words: NiCo2O4, surfactant, solid state reaction, topography

CLC Number:

O614

ZHUANG Jia,CHI Yan-Hua,WANG Dong. Preparation of Different Topography NiCo₂O₄ with Surfactant by Solid[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2007.00040.

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Preparation of Different Topography NiCo₂O₄ with Surfactant by Solid

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