Preparation of AlN Powder by Microwave Carbon Thermal Reduction

doi:10.3724/SP.J.1077.2009.00755

Abstract

Abstract: Aluminium nitride powders were prepared by microwave carbon thermal reduction method. The effects of aluminium sources, carbon sources and additives on AlN powder structure and morphology were studied. XRD analysis shows that most suitable aluminum source and carbon source are selected to be as aluminum hydroxide and acetylene black, respectively. The catalysis effect of additive A on nitridation is most obvious. Industry aluminum hydroxide and acetylene black are completely converted into AlN by adding additive A and heating at 1300℃ for 1h in nitrogen atmosphere. The results show that microwave carbon thermal reduction can reduce the reaction temperate and shortened the reaction time for the preparation of nitride powder.

Key words: microwave carbon thermal reduction, addictive, AlN powder

CLC Number:

TQ174

XIAO Jin,ZHOU Feng,CHEN Yan-Bin. Preparation of AlN Powder by Microwave Carbon Thermal Reduction[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2009.00755.

References

［1］Sheppard L M. Am. Ceram. Soc. Bull., 1990, 69(11): 1801-1812.
［2］Tummala R. J. Am. Ceram. Soc., 1991, 74(5): 895-907.
［3］Kuang JiaCai, Zhang ChangRui, Zhou XinGui, et al. Materials Letters, 2005, 59(16): 2006-2010.
［4］李鹏亮, 周敬恩, 席生岐(LI Peng-Liang, et al). 无机材料学报(Journal of Inorganic Materials), 2006, 21(4): 821-827.
［5］王超, 彰超群, 王日初, 等. 中国有色金属学报, 2007, 17(11): 1729-1738.
［6］Takayuki Ide, Katsutoshi Komeya, Takeshi Meguro, et al. J. Am. Ceram. Soc., 1999, 82(11): 2993-2998.
［7］Jung WooSik, Joo Hyeong Uk. Journal of Crystal Growth, 2005, 285(4): 566-571.
［8］林枞，许业文，徐政. 硅酸盐通报, 2006, 25(3): 132-135.
［9］Ramesh Peelamedu D, Rao Kalya J. Advanced Materials, 1995, 7(2): 177-179.
［10］Vaidhyanathan B, Agrawal D K, Roy R. Journal of Materials Research, 2000, 15(4): 974-981.
［11］王柳燕, 张宁. 粉末冶金工业, 2008, 18(3): 42-46.
［12］匡加才, 张长瑞, 周兴贵, 等. 宇航材料工艺, 2003, 33(5): 44-47.
［13］邱雨, 高濂(QIU Yu, et al). 无机材料学报(Journal of Inorganic Materials), 2004, 19(1): 69-74.
［14］秦明礼, 林健凉, 肖平安, 等(QIN Ming-Li, et al). 无机材料学报(Journal of Inorganic Materials), 2002, 17(5): 1054-1058.
［15］Sakurai T, Yamada O, Miyamoto Y. Materials Science and Engineering, 2006, 416(1/2): 40-44.
［16］戴长虹, 张显鹏, 张劲松, 等. 金属学报, 1996, 32(10): 1221-1226.
［17］Medraj M, Baik Y, Thompson W T, et al. Journal of Materials Processing Technology, 2005, 161(3): 415-422.
［18］Kuang JiaCai, Zhang ChangRui, Zhou XinGui, et al. Journal of Crystal Growth, 2004, 263(1-4): 12-20.
［19］Jung Woo-Sik, Joo Hyeong Uk. Journal of Crystal Growth, 2005, 285(4): 566-571.
［20］Sutton W H. Ceram. Trans., 1993, 36(5): 3-8.
［21］Binner J. Journal of Materials Science Letters, 2002, 21(3): 247-250.
［22］周和平, 陈浩, 吴音, 等. 材料研究学报, 1998, 12(1): 25-30.
［23］曾小锋, 彭虎, 钱端芬, 等. 硅酸盐通报, 2006, 25(4): 36-40.

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