Journal of Inorganic Materials

• Research Paper • Previous Articles     Next Articles

Fabrication of Transparent β-Ca3(PO4)2 Bioceramics by Spark Plasma Sintering Technique using Ultrafine Powders

LIN Kai-Li, QIN Chao, NI Si-Yu, CHEN Li-Dong, LU Jian-Xi, CHANG Jiang   

  1. Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • Received:2005-06-22 Revised:2005-09-22 Published:2006-05-20 Online:2006-05-20

Abstract: Ultrafine powders of β-tricalcium (β-Ca3(PO4)2, β-TCP) powders (about 100nm in average size) were obtained by the precipitation method. Transparent β-TCP bioceramics were fabricated by using these ultrafine powders and spark plasma sintering technique at 875℃ for 2min under 40MPa and at the heating rate of 150℃/min. No phases other than β-TCP were detected in the sintered samples. The relative density of the prepared β-TCP was over 99.7%. The results of the FESEM show that the transparent bodies have an average grain size of 250nm and seem to be pore-free. The MTT method shows that the proliferation of bone mesenchymal stem cells on transparent β-TCP bioceramics is much better than that on the polystyrene cell culture cluster.

Key words: nano, ultrafine powders, \beta-tricalcium phosphate, spark plasma sintering, transparent bioceramics

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