Journal of Inorganic Materials ›› 2022, Vol. 37 ›› Issue (8): 809-820.DOI: 10.15541/jim20220014
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Received:
2022-01-11
Revised:
2022-03-03
Published:
2022-08-20
Online:
2022-03-10
About author:
WANG Shiwei (1964-), male, professor. E-mail: swwang51@mail.sic.ac.cn
Supported by:
CLC Number:
WANG Shiwei. Progress of Spontaneous Coagulation Casting of Ceramic Slurries Based on Hydrophobic Interaction[J]. Journal of Inorganic Materials, 2022, 37(8): 809-820.
Fig. 1 Schematic diagram of ceramic particles solidified by three-dimensional organic network (a) and photo of translucent Al2O3 sheet (100 mm × 100 mm × 1 mm) (b)
Fig. 2 Simplified structure of PIBM molecule (a) and schematic diagrams of organic network with low and high density by spontaneous coagulation casting (b) and gelcasting (c), respectively
Fig. 4 Effect of hydrophobic groups on spontaneous coagulation (a) Hydrophobic modification reaction; (b) Schematic diagram of ceramic particle dispersion and hydrophobic association curing mechanism
Organic ammonium salt | Molecular weight | Solubility of Isobam after hydrophobic modification |
---|---|---|
TMAC (Tetramethyl ammonium chloride) | 109.6 | Soluble |
TEAC (Tetraethylammonium chloride) | 165.7 | Soluble |
MTAC (Methyltributylammonium chloride) | 235.8 | Soluble |
OTAC (Octyltrimethylammonium chloride) | 207.8 | Insoluble |
DTAC (Dodecyltrimethylammonium chloride) | 263.0 | Insoluble |
Table 1 Dissolution of Isobam 600 AF after different hydrophobic chain modification
Organic ammonium salt | Molecular weight | Solubility of Isobam after hydrophobic modification |
---|---|---|
TMAC (Tetramethyl ammonium chloride) | 109.6 | Soluble |
TEAC (Tetraethylammonium chloride) | 165.7 | Soluble |
MTAC (Methyltributylammonium chloride) | 235.8 | Soluble |
OTAC (Octyltrimethylammonium chloride) | 207.8 | Insoluble |
DTAC (Dodecyltrimethylammonium chloride) | 263.0 | Insoluble |
Fig. 7 Schematic diagram of stabilized foam with hydrophobized ceramic particles (a) and corresponding magnification part (showing a modified dispersant on a particle) (b)
Fig. 8 Pictures of wet green bodies before (a) and after (b) joining, and effect of syneresis time on flexural strength of sintered samples (1600 ℃×2 h) derived from wet green bodies (c) [54]
Fig. 10 Density difference of ceramic green bodies prepared by different dispersion systems (a) and photos of sintered samples (280 mm×130 mm×20 mm)(b)[56]
Fig. 12 Schematic diagram of orientation of the platelet under shear flow (a), surface of the green body with platelet (b), XRD patterns of the green bodies sintered at different temperatures (c), and the influence of the content and type of the platelet on the linear transmittance of the ceramic (1 mm thick) (d)[61]
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