Journal of Inorganic Materials ›› 2022, Vol. 37 ›› Issue (8): 841-852.DOI: 10.15541/jim20220002
Special Issue: 2022年度中国知网高下载论文
• REVIEW • Previous Articles Next Articles
CHEN Yongqiang1(), WANG Yixue1, ZHANG Fan1,2, LI Hongxia1,3, DONG Binbin4, MIN Zhiyu4, ZHANG Rui1,4(
)
Received:
2022-01-04
Revised:
2022-03-08
Published:
2022-08-20
Online:
2022-03-29
Contact:
ZHANG Rui, professor. E-mail: zhangray@zzu.edu.cnAbout author:
CHEN Yongqiang (1991-), male, PhD, lecturer. E-mail: chenyq@zzu.edu.cn
Supported by:
CLC Number:
CHEN Yongqiang, WANG Yixue, ZHANG Fan, LI Hongxia, DONG Binbin, MIN Zhiyu, ZHANG Rui. Preparation of Special Ceramics by Microwave Heating: a Review[J]. Journal of Inorganic Materials, 2022, 37(8): 841-852.
Fig. 2 Schematic diagram of the insulation structure of α-Al2O3 powder prepared by microwave pyrolysis[44] (1—High alumina lightweight mullite foam brick head cover; 2—95 alumina crucible; 3—High alumina lightweight mullite foam brick insulation cylinder; 4—SiC auxiliary heating rods; 5—Infrared thermometer hole)
Fig. 3 SEM images of samples obtained from microwave pyrolysis of two precursor powders at different temperatures [44] (a) Aluminum ammonium sulfate dodecahydrate as prcursor, (b) Aluminum hydroxide as precursor
Fig. 4 SEM images of zirconia powders obtained at different microwave pyrolysis temperatures and conventional pyrolysis at 750 ℃[45] (a) 700 ℃; (b) 750 ℃; (c) 800 ℃; (d) 850 ℃; (e) 900 ℃; (f) conventional pyrolysis at 750 ℃
Fig. 6 SEM images of the synthesized SiC crystals by microwave heating at 1100 ℃ and holding for 30 min[56] (a) Spatial growth of SiC crystals; (b) SiC transistors; (c) SEM images of SiC whiskers at (c) low magnification and (d) high magnification
Fig. 10 SEM images of ZTA ceramics doped with different molar contents of La2O3[31] (a-d) Microwave sintering at 1550℃ for 30 min at La2O3 content of (a) 0, (b) 1.5%, (c) 3%, and (d) 5%; (e) Conventional sintering at 1600℃ for 3 h at La2O3 content of 1.5%
Fig. 11 Fracture morphologies of Al2O3-SiC (~5 μm) specimens sintered by microwave at different temperatures[86] (a) 1350 ℃; (b) 1400 ℃; (c) 1450 ℃; (d) 1500 ℃
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