Journal of Inorganic Materials ›› 2022, Vol. 37 ›› Issue (3): 303-309.DOI: 10.15541/jim20210569
• RESEARCH ARTICLE • Previous Articles Next Articles
WANG Yaning1(), ZHANG Yuqi1, SONG Suocheng2, CHEN Ruomeng1,3, LIU Yaxiong4(), DUAN Yugang1
Received:
2021-09-15
Revised:
2021-10-12
Published:
2022-03-20
Online:
2021-12-24
Contact:
LIU Yaxiong, professor. E-mail: yaxiongliu@163.com
About author:
WANG Yaning (1989-), male, PhD candidate. E-mail: 905488248@qq.com
Supported by:
CLC Number:
WANG Yaning, ZHANG Yuqi, SONG Suocheng, CHEN Ruomeng, LIU Yaxiong, DUAN Yugang. Laser Stereolithography for Zirconia Ceramic Fabrication and Its Debinding and Sintering Process[J]. Journal of Inorganic Materials, 2022, 37(3): 303-309.
Component | Mass percentage/% |
---|---|
Bifunctional monomer (HDDA, Curease, China) | 38.0 |
Trifunctional monomer (TMPTA, Curease, China) | 28.5 |
Hexafunctional monomer (DPHA, Curease, China) | 28.5 |
Oligomer (NeoRadU Curease, China) | 5.0 |
Table 1 Component proportion of hybrid resin
Component | Mass percentage/% |
---|---|
Bifunctional monomer (HDDA, Curease, China) | 38.0 |
Trifunctional monomer (TMPTA, Curease, China) | 28.5 |
Hexafunctional monomer (DPHA, Curease, China) | 28.5 |
Oligomer (NeoRadU Curease, China) | 5.0 |
Component | Proportion |
---|---|
Zirconia powder | Volume ratio to resin: 11 : 9 |
Resin | Volume ratio to ceramic: 9 : 11 |
Photoinitiator (819, Curease, China) | 0.3% (mass percentage) of resin |
Dispersant (TEGO685, TEG, China) | 2% (mass percentage) of ceramic |
Defoamer (TEGO900, TEG, China) | 1% (mass percentage) of resin |
Table 2 Component proportion of ceramic slurry
Component | Proportion |
---|---|
Zirconia powder | Volume ratio to resin: 11 : 9 |
Resin | Volume ratio to ceramic: 9 : 11 |
Photoinitiator (819, Curease, China) | 0.3% (mass percentage) of resin |
Dispersant (TEGO685, TEG, China) | 2% (mass percentage) of ceramic |
Defoamer (TEGO900, TEG, China) | 1% (mass percentage) of resin |
Fig. 3 Horizontal dimension error vs. scanning line space (a), schematic diagram of scanning strategy (b), horizontal dimension error vs. scanning line width compensation (c), and stacking dimension error vs. slicing thickness (d)
Fig. 4 TG and DTG curves of different resin in different atmosphere (a), debinding curve of green body (b), pictures of strip parts after debinding in nitrogen (c) and air (d) atmospheres, and SEM images of green part (e) and debinded part (f) Colorful figures are availuable on the website
Fig. 5 Sintering curve (a), pictures of green parts of cube (b) and three units dental bridge (c), sintered parts of cube (d) and three units dental bridge (e), and SEM image of sintered part (f)
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