Journal of Inorganic Materials ›› 2016, Vol. 31 ›› Issue (1): 47-52.DOI: 10.15541/jim20150142
• Orginal Article • Previous Articles Next Articles
TAN Xiao-Ping1, QI Li-Ping1, 2, LIANG Shu-Quan1
Received:
2015-03-23
Revised:
2015-05-28
Published:
2016-01-20
Online:
2015-12-15
CLC Number:
TAN Xiao-Ping, QI Li-Ping, LIANG Shu-Quan. Effect of La, Y Additions on ZrO2-mullite Nano-composite Ceramics by In-situ Controlled Crystallizing from Si-Al-Zr-O Amorphous Bulk[J]. Journal of Inorganic Materials, 2016, 31(1): 47-52.
No. | SiO2 | Al2O3 | ZrO2 | Y2O3 | La2O3 | MgO+CaO |
---|---|---|---|---|---|---|
Z3 | 35 | 40 | 20 | 0 | 0 | 5 |
ZY1 | 35 | 40 | 20 | 0.5 | 0 | 5 |
ZY2 | 35 | 40 | 20 | 1.0 | 0 | 5 |
ZY3 | 35 | 40 | 20 | 2.0 | 0 | 5 |
ZY4 | 35 | 40 | 20 | 4.0 | 0 | 5 |
ZYL0(ZY2) | 35 | 40 | 20 | 1.0 | 0 | 5 |
ZYL1 | 35 | 40 | 20 | 1.0 | 0.6 | 5 |
ZYL2 | 35 | 40 | 20 | 1.0 | 1.2 | 5 |
ZYL3 | 35 | 40 | 20 | 1.0 | 1.8 | 5 |
Table 1 Composition of the samples in the study(wt%)
No. | SiO2 | Al2O3 | ZrO2 | Y2O3 | La2O3 | MgO+CaO |
---|---|---|---|---|---|---|
Z3 | 35 | 40 | 20 | 0 | 0 | 5 |
ZY1 | 35 | 40 | 20 | 0.5 | 0 | 5 |
ZY2 | 35 | 40 | 20 | 1.0 | 0 | 5 |
ZY3 | 35 | 40 | 20 | 2.0 | 0 | 5 |
ZY4 | 35 | 40 | 20 | 4.0 | 0 | 5 |
ZYL0(ZY2) | 35 | 40 | 20 | 1.0 | 0 | 5 |
ZYL1 | 35 | 40 | 20 | 1.0 | 0.6 | 5 |
ZYL2 | 35 | 40 | 20 | 1.0 | 1.2 | 5 |
ZYL3 | 35 | 40 | 20 | 1.0 | 1.8 | 5 |
No. | Tp1/℃ | Tp2 /℃ |
---|---|---|
Z3 | 1007 | 1174 |
ZY1 | 1004 | 1172 |
ZY2 | 1007 | 1174 |
ZY3 | 1009 | 1170 |
ZY4 | 1015 | 1167 |
ZYL1 | 1008 | 1172 |
ZYL2 | 1006 | 1170 |
ZYL3 | 1004 | 1168 |
Table.2 Top temperatures on the DSC curves of samples with the additives of La2O3 and Y2O3
No. | Tp1/℃ | Tp2 /℃ |
---|---|---|
Z3 | 1007 | 1174 |
ZY1 | 1004 | 1172 |
ZY2 | 1007 | 1174 |
ZY3 | 1009 | 1170 |
ZY4 | 1015 | 1167 |
ZYL1 | 1008 | 1172 |
ZYL2 | 1006 | 1170 |
ZYL3 | 1004 | 1168 |
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