Journal of Inorganic Materials ›› 2012, Vol. 27 ›› Issue (12): 1331-1335.DOI: 10.3724/SP.J.1077.2012.12123

• Research Paper • Previous Articles     Next Articles

Study on the Consolidation Process of Protein Foaming in the Preparation of Ceramic Foams

YIN Liu-Yan, ZHOU Xin-Gui, YU Jin-Shan, ZHAO Shuang, LUO Zheng, YANG Bei   

  1. (National Key Laboratory of Science and Technology on Advanced Ceramic Fibers and Composites, National University of Defense Technology, Changsha 410073, China)
  • Received:2012-03-01 Revised:2012-05-04 Published:2012-12-20 Online:2012-11-19
  • About author:YIN Liu-Yan. E-mail: hanqing421720@sina.com
  • Supported by:

    National Natural Science Foundation of China (E020301)

Abstract: High porosity Si3N4 ceramic foams were fabricated by protein foaming method using egg white protein as foam agents. Atmosphere-, constant- and high-pressure consolidation processes were tested to prepare ceramic foams. The effects of air pressure on cellular structure, open porosity and pore size distribution of the as-prepared ceramic foams were investigated. The results showed that ceramic foams with average pore size and porosity of  210 μm and 78.6% was obtained by constant-pressure consolidation, which are the highest values among all the three groups. Moreover, SEM reveals that ceramic foams with uniformly ellipsoidal pores are produced by atmosphere- and constant-pressure consolidation processes, while ceramic foams with regular sphere pores are produced by high-pressure consolidation. The walls’ thickness of the pores increase with the increase of air pressure during consolidation process. As a result, the high-pressure consolidation process yields the highest compressive strength (nearly 50 MPa) of ceramic foams.

Key words: protein foaming, ceramic foams, Si3N4, consolidation

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