Crystallization Kinetics of BaO-Al2O3-SiO2 Glass-ceramics

doi:10.3724/SP.J.1077.2008.00315

Abstract

Abstract: BaO-Al2O3-SiO2(BAS) glass-ceramics with stoichiometric and off-stoichiometric celsian composition were fabricated. Crystallization characters of two groups of BaO-Al₂O₃-SiO₂ (BAS) glass-ceramics were investigated by differential scanning calorimetry (DSC), X-ray diffraction(XRD), isoconversional method and multiple linear regression method. The autocatalytic kinetic model (Sest\acute ak-Berggren function) was found to be the most proper description of the studied processes for all glass investigated. Doping with ZrO₂ or increasing mass fraction of BaO accelerates the crystallization process of hexagonal-BaAl₂Si₂O₈ in BAS glass-ceramics with stoichiometric celsian composition whose viscosity is high. Moreover, the lower the temperature gets, or the higher the crystallinity gets, the more obvious the accelerating effect gets. While doping with ZrO₂ decelerates the crystallization process of hexagonal-BaAl₂Si₂O₈ in BAS glass-ceramics with off-stoichiometric celsian composition whose viscosity is low. Moreover, the higher the temperature gets, the more obvious the decelerating effect gets.

Key words: glass-ceramics, celsian, crystallization, isoconversional method, Sestacute ak-Berggren function

CLC Number:

TG171

LU Yu-Feng,DU Yong-Guo,XIAO Jia-Yu,ZHANG Wei-Jun,ZHENG Xiao-Hui,ZHOU Wen-Yuan. Crystallization Kinetics of BaO-Al₂O₃-SiO₂ Glass-ceramics[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2008.00315.

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Crystallization Kinetics of BaO-Al₂O₃-SiO₂ Glass-ceramics

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