Journal of Inorganic Materials

• Research Paper • Previous Articles     Next Articles

Fabrication of YAG Transparent Ceramics by Two Step Sintering Process

CHEN Zhi-Hui 1,2, LI Jiang-Tao 2, HU Zhang-Gui 2, XU Jiu-Jun 3   

  1. 1. Graduate University of the Chinese Academy of Sciences, Beijing 100049, China; 2. Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100080, China; 3. Dalian Maritime University, Dalian 116026, China
  • Received:2007-02-08 Revised:2007-04-19 Published:2008-01-20 Online:2008-01-20

Abstract: Well dispersed yttrium aluminum garnet (YAG) nanopowders with mean particle size of about 50nm synthesized by modified co-precipitation method were used to sinter YAG transparent ceramics with 0.5wt% TEOS as sintering additive by two step sintering process. The samples were first heated to a higher temperature ranging from 1700℃ to 1800℃, then cooled down to a lower temperature ranging from 1500℃ to 1600℃, and held at the lower temperature for 10h. Grain-boundary migration is suppressed and grain-boundary diffusion is promoted during the two step sintering process. When the two step sintering temperatures are 1800℃ and 1550℃, the microstructure of YAG is homogeneous with average grain size of 6μm without abnormal grain growth and the transmittance of the specimen is 72.0%

Key words: two-step sintering process, YAG, transparent ceramics

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