Preparation of MnV2O6 Nanoflakes via Simple Hydrothermal Process

doi:10.3724/SP.J.1077.2007.01139

Abstract

Abstract: Single-phase monoclinic MnV₂O₆ nanoflakes were prepared by the hydrothermal process at 180℃ for 18h, using Mn(CH₃COO)₂·4H ₂O and NH₄VO₃ as starting materials, and acetic acid was used to adjust the pH value of the reaction solution. The as-prepared samples were characterized by field emission scanning electron microscope (FESEM), and transmission electron microscope (TEM), X-ray photoelectron spectrum measurements, and the component of MnV₂O₆ was confirmed. The result indicates that the products consist of a large quantity of compact accumulated nanoflakes, with average width of 0.85μm, thickness of 100nm and lengthup to 1.7μm.

Key words: MnV₂O₆, hydrothermal synthesis, nanoflakes

CLC Number:

O648

LIU Yi,Qian Yi-Tai. Preparation of MnV₂O₆ Nanoflakes via Simple Hydrothermal Process
[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2007.01139.

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Preparation of MnV₂O₆ Nanoflakes via Simple Hydrothermal Process

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