Journal of Inorganic Materials

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SiC Nanowires Synthesized by Microwave Heating

LU Bin, LIU Ji-Xuan, ZHU Hua-Wei, JIAO Xian-He   

  1. (School of Materials Science and Engineering, Central South University, Changsha 410083, China)

  • Received:2006-11-21 Revised:2006-12-26 Published:2007-11-20 Online:2007-11-20

Abstract: Large-scale silicon carbide nanowires were prepared by using pure silicon powder and phenolic resin, which were mixed, molded, carbonizated, and then subjected to the microwave heating with a rate of 10℃/min between 1300℃ and 1400℃ in the static argon atmosphere for 0.5--2h. The SiC nanowires were characterized by means of SEM and TEM, the composition of samples were determined through EDX. The prepared nanowires show a core-shell structure with diameters ranging from 20nm to 100 nm. The results show that liquid silicon acts as catalyst and key raw material for preparing SiC nanowires.

Key words: silicon carbide, nanowire, phenol formaldehyde resin, microwave heating

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