Synthesis and Characterization of SnO2 Nanobelts by Carbothermal\\ Reduction of SnO2 Powder

doi:10.3724/SP.J.1077.2007.00609

Abstract

Abstract: The mixture of SnO₂ powder and graphite was ground to ensure complete mixing, and was put into an alumina boat, then this boat was placed in the hot zone of the tube, heated from room temperature to 1100℃ and kept at this temperature for 2.5h in flowing argon. The X-ray diffraction analysis (XRD) indicates that the nanobelts are tetragonal rutile structure of SnO₂. Scaning electron microscope(SEM) and transmission electron microscope(TEM) observations reveal that the nanobelts are uniform. The selected-area electron diffraction analysis(SAED) demonstrates that the nanobelts are single crystal . The SnO₂ nanobelts might grow via a vapor-solid(VS) process.

Key words: tin dioxide, nanobelt, quasi-one dimensional nanostructure, vapor-solid(VS) process

CLC Number:

O469

NI Zi-Feng,YING Peng-Zhan,LUO Yong,DAI Xin-Lian,LIU Tao. Synthesis and Characterization of SnO₂ Nanobelts by Carbothermal\\ Reduction of SnO2 Powder[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2007.00609.

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Synthesis and Characterization of SnO₂ Nanobelts by Carbothermal\\ Reduction of SnO2 Powder

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