Journal of Inorganic Materials

• Research Paper • Previous Articles     Next Articles

Fabrication of SiC Whisker Reinforced Laminated Si3N4 /BN Ceramics by Spark Plasma Sintering

LI Cui-Wei; HUANG Yong; WANG Chang-An; TANG Ke; LI Shu-Qin   

  1. State key Lab of New Ceramics and Fine Processing; Department of Materials Science and Engineering; Tsinghua University; Beijing 100084; China
  • Received:2001-09-24 Revised:2001-11-30 Published:2002-11-20 Online:2002-11-20

Abstract: SiC whisker reinforced laminated Si3N4/BN ceramics with additives Y2O3, Al2O3 and MgO were prepared by spark plasma sintering(SPS) in 13min of heating
to 1650℃ and 15min dwell time. The density of the samples densified by SPS was 3.18g/cm3. Bending strength reached 600 MPa, and the work of fracture
reached 3500 J/m2. The arrangement of hard Si3N4 layer and soft BN layer, the pull-out and broken of SiC whisker were the main reason for improving toughness
of this ceramic. XRD and SEM indicated SiC whisker, long rod like β-Si3N4 and platelet like hex-BN were the main phase and SiC whisker, long rod like β-Si3N4 had strong preferred orientation.

Key words: SPS, laminated ceramics, Si3N4

CLC Number: