Journal of Inorganic Materials

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Applications of X-ray Fluorescence Spectrometry in Elemental Analysis of Crystals

ZHUO Shang-Jun; TAG Guang-Yi; JI Ang; SHENG Cheng; SHEN Ru-Xiang   

  1. Shanghai Institute of Ceramics; Chinese Academy of Sciences; Shanghai 200050; China
  • Received:2001-12-30 Revised:2002-02-26 Published:2003-01-20 Online:2003-01-20

Abstract: The applications of X-ray fluorescence spectrometry in elemental analysis of crystals were
reviewed. Although it is an effective and efficient approach for elemental analysis, X-ray fluorescence analyses require different sample preparation
methods depending on different sample types and require calibration standards to correct matrix effects. Abnormal reflection may lead to
complicated background and confused qualitative interpretation or/and quantitative measuring conditions if the measured specimen is a single
crystal. In this case, the fusion method is preferable. Attention must be paid to the uncertainty of the measurement when the results are employed
to a specific purpose.

Key words: X-ray fluorescence spectrometry, crystal, quantitative analysis, uncertainty of mea- surement

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