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无机材料学报

无机材料学报

• 研究论文 • 上一篇    

氧化铅的添加对激光诱导玻璃中金纳米颗粒析出的影响

曾惠丹; 邱建荣; 姜雄伟; 朱从善; 干福熹   

  1. 中国科学院上海光学精密机械研究所中日合作“Photon Craft Project”实验室 上海; 201800
  • 收稿日期:2003-02-21 修回日期:2003-05-08 出版日期:2004-03-20 网络出版日期:2004-03-20

Effect of PbO on Precipitation of Laser-induced Au Nanoparticles Inside Glasses

ZENG Hui-Dan; QIU Jian-Rong; JIANG Xiong-Wei; ZHU Cong-Shan; GAN Fu-Xi   

  1. Photon Craft Project; Shanghai Institute of Optics and Fine Mechanics; Chinese Academy of Sciences; and Japan Science and Technology Corporation; Shanghai 201800; China
  • Received:2003-02-21 Revised:2003-05-08 Published:2004-03-20 Online:2004-03-20

PDF (PC)

1082

被引次数

10

摘要： 使用飞秒激光辐照和热处理相结合,通过引入PbO,实现了在含有金离子的硅酸盐玻璃内部,有空间选择性地析出大尺寸金纳米颗粒.通过吸收光谱,电子自旋共振谱和透射电镜测试研究了氧化铅对激光诱导金纳米颗粒析出的影响.实验结果表明,氧化铅的引入能抑制空穴捕获型色心生成,并促进金纳米颗粒的长大.

关键词: 飞秒激光, 金纳米颗粒, 氧化铅, 硅酸盐玻璃

Abstract: Three-dimensional precipitation of large size Au nanoparticles in gold ion-doped silicate glasses was achieved by a femtosecond laser irradiation and successive heat treatment. The effects of PbO on the precipitation of Au nanoparticles were investigated by means of optical absorption, electron spin resonance spectra and TEM. The experimental results show that, introducing PbO results in inhibition of hole-trapped centers induced by femtosecond laser irradiation, and promotion of the formation and growth of Au nanoparticles.

Key words: femtosecond laser, Au nanoparticles, PbO, silicate glass

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