Investigation on Crystallization Behavior of Y2O3-Al2O3-SiO2 Glass Prepared by High-gravity Combustion Synthesis

doi:10.3724/SP.J.1077.2013.12592

Abstract

Abstract: The crystallization behavior of Y₂O₃-Al₂O₃-SiO₂ glass prepared by high-gravity combustion synthesis was investigated by isothermal annealing experiments. The effect of annealing condition on the crystallization behavior of the glass was discussed according to the Y₂O₃-Al₂O₃-SiO₂ternary phase diagram. From experimental results, the crystallization behavior of the glass strongly depended on the annealing temperature and the content of SiO₂. After being annealed at 1050℃, the sample showed a graded phase distribution along the high-gravity direction, consisting of Al₆Si₂O₁₃ glass-ceramic, pure glass and χ-Al₂O₃ glass-ceramic. At annealing temperature of 1100℃, Y₃Al₅O₁₂ and Y₂Si₂O₇ were precipitated as the major crystalline phases. When the annealing temperature further increased to 1200℃, the predominant crystalline phase was Y₃Al₅O₁₂. The research provides a possible way to prepare Y₂O₃-Al₂O₃-SiO₂ glass-ceramics by integrating high-gravity combustion synthesis with post annealing treatment.

Key words: high-gravity combustion synthesis, Y₂O₃-Al₂O₃-SiO₂ glass, annealing, crystallization

CLC Number:

TB321

YANG Zeng-Chao, LIU Guang-Hua, XU Li-Hua, LI Jiang-Tao, GUO Shi-Bin. Investigation on Crystallization Behavior of Y₂O₃-Al₂O₃-SiO₂ Glass Prepared by High-gravity Combustion Synthesis[J]. Journal of Inorganic Materials, 2013, 28(7): 780-784.

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Investigation on Crystallization Behavior of Y₂O₃-Al₂O₃-SiO₂ Glass Prepared by High-gravity Combustion Synthesis

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